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10-17
Columns:150x4.6mmEluent:MeCN/50mMKH2PO450/50,pH3,Flowrate:1ml/min1:primidone:普里米酮;去氧;撲癇酮2:Phenobarbitone:3:carbamazepine卡馬西平,立痛定;卡巴咪嗪;酰胺咪嗪;氨甲酰氮草
10-17
BeksichSt120BS-C23,(100x4.6mm)流動相:A=0.1%TFA,B=0,1%TFAinACN梯度:15-40%Bin10min.,流速:1ml/min監(jiān)測波長:230nm
10-17
同時分析1-and2-val.陽離子Column:BeksichCat,5um(or7um)(125x4.6mm)Eluent:5.0mM檸檬酸+0.5mM2,6吡啶二甲酸or0.6mM抗壞血酸+3.3mM磷酸pH2,7
10-17
AnioneswithSuppressorColumn:BeksichGelAXS(150x4mm)Eluent:1.7mM碳酸氫鈉/1.8mM碳酸鈉/0.1mM硫氰酸鈉溫度:RT流速:2ml/min.進(jìn)樣量:100ulF:氟離子,Cl:氯離子,Nitrite:亞硝酸鹽,Bromide:溴化物,nitrate;硝酸,Phosphate:磷酸鹽,Sulfate:硫酸Column:BeksichGelAX,10um(150x4mm)Eluent:mM鄰苯二甲酸氫鉀(pH6.0)流...
10-17
Beksich-TG-Chiral,5um(250x3mm),梯度:50mM醋酸緩沖液pH4,5/乙腈(1/1),流速:0,6ml/min檢測器:UV254nm1=D+L-Serin/D+L-絲氨酸2=D+L-纈氨酸3=D+L-色氨酸
10-17
BeksichDABS,4um(200x4.6mm)流動相:A:25mM醋酸鈉pH=6,6/乙腈(80/20),B:乙腈/異丙醇(40/60)梯度:0min.0%B,4min.5%B,8min.20%B,15min.25%B,27min.60%B,28min.100%B,32min.100%B流速:1ml/min.檢測波長:VIS436nm溫度:40℃BeksichFMOC-H,5um(250x4mm)流動相:A:50mM醋酸鈉pH4.2/乙腈(80/20)B=50mM醋酸鈉...
10-17
BeksichSt120BS-C235um(100x4.6mm)流動相:A=0,1%TFA,B=0,1%TFAinACN,梯度:5-100%Bin10min.,流速:1ml/min1:nicotine/煙堿2:quinine/奎寧3:doxepin/多慮平4:amitriptyline/阿米替林5;t-cinnamicacid反肉桂酸6:4-butylbenzoicacid/對丁基苯甲酸7:4-octylbenzoicacid/對辛基苯甲酸
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